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甲醇与氨生产甲胺的测定专用填充柱AM

甲醇与氨生产甲胺的测定专用填充柱AM
  • 甲醇与氨生产甲胺的测定专用填充柱AM
  • 供应商:
    浩瀚色谱(山东)应用技术开发有限公司
  • 价格:
    面议
  • 最小起订量:
    1个
  • 地址:
    山东滕州市(商务部和技术部)
  • 手机:
    13963221227
  • 联系人:
    王经理 (请说在中科商务网上看到)
  • 产品编号:
    214420316
  • 更新时间:
    2024-04-22
  • 发布者IP:
    119.186.201.104
  • 产品介绍
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详细说明

  甲胺是医药、农药、溶剂、染料、树脂、橡胶和炸药的原料,还可用作染料助剂、催化剂、阻聚剂和抗氧剂,用途十分广。

  工业上通常是在氧化铝、氧化硅一氧化铝之类的硅铝催化剂存在下,将甲醇与氨连续反应来制造甲胺。反应一般是在高压和300~500℃温度范围内,在气相中进行。反应产物一甲胺、二甲胺和三甲胺分布接近热力学平衡组成,三甲胺含量最高,一甲胺和二甲胺较低,这类催化剂一般称为平衡型催化剂。由于二甲胺在工业上广泛用作化学中间体,因此,甲醇或二甲醚胺化反应的最主要目的产物是二甲胺。为提高二甲胺产量、降低三甲胺产量,工业上通常采用将多余的三甲胺进行循环、调整原料氮/碳比和应用改进的催化剂。

  名称:甲胺填充柱

  型号:HH-AM

  规格:3m*3mm,60-80目

  *高使用温度:120°C

  编号:20240227001

  应用:工业甲胺,二甲胺,三甲胺的测定 气相色谱法

  HG/T 2974-1999 工业30%三甲胺水溶液

  HG/T 2974-1999 工业30%三甲胺水溶液

  本标准规定了由三甲胺配制成的30%水溶液的要求、采样、试验方法、标志、包装、运输和贮存等。

  本标准适用于由甲醇连续气相催化氨化法生产的三甲胺配制成的30写水溶液。

  浩瀚色谱研制的HH-AM专用柱测定一甲胺,二甲胺,三甲胺,甲醇,水及氨,结果满意。

  Methylamine is a raw material for pharmaceuticals, pesticides, solvents, dyes, resins, rubber, and explosives. It can also be used as a dye additive, catalyst, polymerization inhibitor, and antioxidant, with a wide range of applications.

  In industry, methanol is usually continuously reacted with ammonia to produce methylamine in the presence of silicon aluminum catalysts such as alumina and silica alumina. The reaction is generally carried out in the gas phase under high pressure and a temperature range of 300-500 ℃. The distribution of reaction products such as monomethylamine, dimethylamine, and trimethylamine is close to thermodynamic equilibrium composition, with trimethylamine having the highest content and monomethylamine and dimethylamine having lower content. These types of catalysts are generally referred to as equilibrium catalysts. Due to the widespread use of dimethylamine as a chemical intermediate in industry, the primary target product of methanol or dimethyl ether amination reactions is dimethylamine. In order to increase the production of dimethylamine and reduce the production of trimethylamine, industry usually uses circulating excess trimethylamine, adjusting the nitrogen/carbon ratio of raw materials, and applying improved catalysts.

  Name: Methylamine filled column

  Model: HH-AM

  Specification: 3m * 3mm, 60-80 mesh

  *High operating temperature: 120 ° C

  Number: 20240227001

  Application: Determination of industrial methylamine, dimethylamine, and trimethylamine by gas chromatography

  HG/T 2974-1999 Industrial 30% trimethylamine aqueous solution

  HG/T 2974-1999 Industrial 30% trimethylamine aqueous solution

  This standard specifies the requirements, sampling, testing methods, labeling, packaging, transportation, and storage of a 30% aqueous solution prepared from trimethylamine.

  This standard applies to 30 octane aqueous solutions prepared from trimethylamine produced by continuous gas-phase catalytic amination of methanol.

  The HH-AM dedicated column developed by Haohan Chromatography was used to determine monomethylamine, dimethylamine, trimethylamine, methanol, water, and ammonia with satisfactory results.